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In the title compound, C 12 H 9 N 2+ ·C 7 F 5 O 2− ·2C 7 HF 5 O 2 , the cation and anion are linked by an N—H⋯O hydrogen bond. The neutral mol­ecules bond to the anion  via  O—H⋯O hydrogen bonds to form associations of one cation, one anion and two neutral mol­ecules. Inter­molecular C—H⋯O, C—H⋯F, F⋯F [shortest contact = 2.768 (8) Å], F⋯π [shortest contact = 3.148 (13) Å] and π–π [shortest centroid–centroid separation = 3.689 (5) Å] inter­actions further link the components to form a three-dimensional network.

1,10-Phenanthrolinium 2,3,4,5,6-pentafluorobenzoate–2,3,4,5,6-pentafluorobenzoic acid (1/2)