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In an attempt to synthesize new cobalt(II) sulfate framework structures using 1,4-diaza­bicyclo­[2.2.2]octane as a template, crystals of poly[0.35-[hexa­aqua­cobalt(II)] [tri-μ-hydroxido-μ-sulfato-dicobalt(II)]], {[Co(H 2 O) 6 ] 0.35 [Co 2 (OH) 3 (SO 4 )]}  n  , were obtained as a mixture with [Co(H 2 O) 6 ]SO 4  crystals. The crystal structure can be described as being constructed from discrete brucite-type [Co 4 (OH) 6 (SO 4 ) 2 ] layers, each of which is built up from edge-shared [Co(OH) 6 ] and [Co(OH) 4 (OSO 3 ) 2 ] octa­hedra, with partial inter­calation by [Co(H 2 O) 6 ] 2+  ions. The absence of  ca  30% of the [Co(H 2 O) 6 ] 2+  cations indicates partial oxidation of cobalt(II) to cobalt(III) within the layer.

Intercalated brucite-type layered cobalt(II) hydroxysulfate