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Single crystals of {FeHo 6 }I 12 Ho were obtained during the reaction of HoI 3  with metallic holmium and iron in a sealed tantalum container. The crystal structure consists of isolated holmium clusters encapsulating a single Fe atom, {FeHo 6 } (symmetry). The rare earth metal atoms are surrounded by 12 edge-capping and six terminal iodide ligands that either connect the clusters to each other directly or  via  HoI 6  octa­hedra (symmetry).

Holmium dodecaiodidoiron-octahedro-hexaholmium, {FeHo6}I12Ho

Holmium dodecaiodidoiron-octahedro-hexaholmium, {FeHo₆}I₁₂Ho