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The tripeptide title compound, C 32 H 53 N 3 O 6 , synthesized in 80% yield by coupling of  N -methyl- l -leucine benzyl ester with  tert -butoxy­carbonyl- l -leucyl- N -methyl- l -leucine at 273 K, conjugates through two amide linkages and includes two protecting groups: a  tert -butyl­oxycarbonyl group at the C-tip and a benzyl group at the N-tip. A classical inter­molecular N—H⋯O hydrogen bond and a weak non-conventional inter­molecular C—H⋯O contact connect the mol­ecules, forming layers parallel to (001).

acta crystallographica. section e

N-{N-[N-(1,1-Dimethylethoxycarbonyl)-<scp>L</scp>-leucyl]-N-methyl-<scp>L</scp>-leucyl}-N-methyl-<scp>L</scp>-leucine benzyl ester

N-{N-[N-(1,1-Dimethylethoxycarbonyl)-L-leucyl]-N-methyl-L-leucyl}-N-methyl-L-leucine benzyl ester