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Reaction of [Ru(Tp)Cl(PPh(3))(2)] {where Tp is hydridotri-pyrazol-yl-borate, BH[C(3)H(3)N(2))(3))]} with NH(4)[S(2)P(OEt)(2)] in methanol afforded the title compound, [Ru(C(9)H(10)BN(6))(C(4)H(10)O(2)PS(2))(C(18)H(15)P)], in which the Ru(II) ion is in a slightly disorted octa-hedral coordination environment. The [S(2)P(OEt)(2)](-) ligand coordinates in a chelating mode with two similar Ru-S bond lengths and a slightly acute S-Ru-S angle. The atoms of both -OCH(2)CH(3) groups of the diethyl dithio-phosphate ligand are disordered over two sites with approximate occupancies of 0.76 and 0.24.

acta crystallographica. section e

(O,O′-Diethyl dithiophosphato-κ2S,S′)(hydridotripyrazol-1-ylborato-κ3N2,N2′,N2′′)(triphenylphosphine-κP)ruthenium(II)