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The title dysprosium coordination polymer, {[Dy 2 (C 10 H 8 O 6 ) 3 (H 2 O) 2 ]·2H 2 O}  n  , was synthesized by reacting dysprosium(III) nitrate and the flexible ligand ( p -phenyl­enedi­oxy)diacetic acid under hydro­thermal conditions. Each Dy III  ion is coordinated by nine O atoms in a tricapped trigonal prismatic geometry. The DyO 9  polyhedra form layers parallel to the  bc  plane. The rigid benzene rings of the anions link the layers along the  a  axis, forming a three-dimensional framework.

Poly[[diaquatris[μ4-(p-phenylenedioxy)diacetato]didysprosium(III)] dihydrate]

Poly[[diaquatris[μ₄-(p-phenylenedioxy)diacetato]didysprosium(III)] dihydrate]