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The title compound, [Re 2 (OH)(C 10 H 8 N 2 ) 2 (CO) 6 ][ReO 4 ], is a mixed-valence rhenium compound containing discrete anions and cations. The Re I  atoms are in a slightly distorted octa­hedral environment, whereas the Re VII  atoms show the typical tetra­hedral coordination mode. The dihedral angle between the two bipyridine groups is 34.3 (7)°.

μ-Hydroxido-bis[(2,2′-bipyridine)tricarbonylrhenium(I)] perrhenate