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The title compound, [Os 3 (C 9 H 6 NS)H(CO) 10 ], contains a nearly equilateral triangle of Os atoms. Two of the Os atoms are bridged by an S atom of the quinoline-2-thiol­ate ligand. Ten carbonyl groups complete the cluster, resulting in a distorted octa­hedral geometry for each Os atom. The hydride atom, which was located in a difference Fourier map and refined isotropically, bridges the shortest Os–Os edge.

acta crystallographica. section e

Decacarbonyl-1κ3C,2κ3C,3κ4C-μ-hydrido-1:2κ2H:H-(μ-quinoline-2-thiolato-1:2κ2S:S)diosmium(I)osmium(0)(3Os—Os)