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The title compound, K 4 [Mo VI O 2 (SO 4 ) 3 ], was precipitated from a melt of molybdenum(VI) oxide and potassium sulfate in potassium disulfate. The compound contains monomeric [Mo VI O 2 (SO 4 ) 3 ] 4−  anions, with the Mo VI  atom, both oxide ligands, and the S atom and both ligating O atoms of the bidentate sulfate group lying on a crystallographic mirror plane. One of the potassium cations is nine-coordinate, while the other is eight-coordinate.

Tetrapotassiumcis-dioxido-trans-bis(sulfato-κO)sulfato(κ2O,O′)molybdate(VI)

Tetrapotassiumcis-dioxido-trans-bis(sulfato-κO)sulfato(κ²O,O′)molybdate(VI)