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The title compound, [Yb 2 (CF 3 O 3 S)(C 10 H 15 ) 2 (OH) 2 (C 12 H 12 N 2 ) 2 ](C 24 H 20 B)·C 12 H 12 N 2 , crystallizes as a half-sandwich complex with a bridging trifluoro­methane­sulfonate as well as two bridging hydroxide groups. The bound bipyridine ligands have N—C—C—N torsion angles of 13.1 (9) and −12.1 (8)°. The structure also contains an uncoordinated 5,5′-dimethyl-2,2′-bipyridine molecule with an N—C—C—N torsion angle of 169.5 (7)°. The triply bridged Yb centers are 3.5990 (4) Å apart. The Yb—N bond lengths are in the range 2.389 (6)–2.424 (5) Å.

acta crystallographica. section e

Di-μ-hydroxido-κ4O:O-μ-trifluoromethanesulfonato-κ2O:O′-bis[(5,5′-dimethyl-2,2-bipyridine-κ2N,N′)(η5-pentamethylcyclopentadienyl)ytterbium(III)] tetraphenylborate 5,5′-dimethyl-2,2-bipyridine