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Single crystals of [Dy10Br18(C2)2] were obtained during the reaction of DyBr3 with dysprosium metal and graphite in a sealed tantalum container. In the crystal structure, the Dy atoms form dimers of edge-sharing octahedra, each encapsulating a C2 unit. The metal atoms are surrounded by Br atoms above the cluster edges and vertices, respectively. The dimers are connected to each other by Br atoms, leading to a three-dimensional network. [Dy10Br18(C2)2] is isotypic with its iodido analogue [Dy10I18(C2)2]

Octadecabromidobis(dicarbido)decadysprosium, [Dy10Br18(C2)2]

Octadecabromidobis(dicarbido)decadysprosium, [Dy₁₀Br₁₈(C₂)₂]