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The title compound, [Fe3(C8H8N2O)S2(CO)8], was prepared by the direct reaction of Fe3(CO)12 and 5-methoxy-1H-benzoimidazole-2-thiol in tetrahydrofuran. Desulfurization took place readily to form a sulfide carbonyl cluster. The molecule contains a triangle consisting of three Fe atoms capped by two S atoms above and below. There are two Fe&#8212;Fe bonds [2.6322&#8197;(5) and 2.5582&#8197;(5)&#8197;&#197;] in the triangle; the length of the third edge [3.3987&#8197;(5)&#8197;&#197;] is too long to represent an Fe&#8212;Fe bond

Octacarbonyl(5-methoxy-2,3-dihydro-1H-benzimidazol-2-yl)di-μ3-sulfido-diiron(I)iron(II)(2Fe—Fe)

Octacarbonyl(5-methoxy-2,3-dihydro-1H-benzimidazol-2-yl)di-μ₃-sulfido-diiron(I)iron(II)(2Fe—Fe)