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The title complex, [Ni2(C42H46Cl2N6O2)(C2H3O2)]ClO4&#183;2CH3CN, was synthesized by condensation of 2,6-diformyl-4-chlorophenol with N,N-bis(aminopropyl)benzylamine in the presence of NiII ions. The ligand is a 28-membered macrocycle with two identical pendant arms. The coordination geometries of the Ni atoms are both octahedral. The two Ni atoms are bridged by two phenolate O atoms of the macrocyclic ligand and one acetate ligand, with an Ni...Ni distance of 3.147&#8197;(4)&#8197;&#197;

acta crystallographica. section e

μ-Acetato-κ2O:O′-[7,23-dibenzyl-15,31-dichloro-3,7,11,19,23,27-hexaazatricyclo[27.3.1.113,17]tetratriconta-1(32),2,11,13,15,17(34),18,27,29(33),30-decaene-33,34-diolato-κ10N4,N5,N6,O1,O2:N1,N2,N3,O1,O2]dinickel(II) perchlorate acetonitrile disolvate