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order on the 2-20 nm scale were discovered. Secondly, a complex cubic phase of some polycatenar LCs (rod-like molecules with more than one appended terminal chain) is investigated. Thirdly, packing of gold nanoparticles coated with nematogens is studied. Powder, single domain and fibre patterns are used, as appropriate, with GISAXS proving particularly useful. Electron density reconstruction is used routinely, but to help solve the phase problem a number of methods are used, including different variants of isomorphous replacement, model building and refinement, and supporting neutron scattering experiments. The main conclusion is that, with the ever increasing complexity of liquid crystal phases, the simple comparison of spacings and molecular dimensions as a method of structural characterization, often used in the past, is increasingly becoming a thing of the past. 1. G Ungar, XB Zeng, Soft Matter, 2005, 1, 95. 2. Prehm, M,, Liu, F., Baumeister, U., Zeng, X.B., Ungar, G., Tschierske, C. Angew. Chem. Int. Ed., 2007, 46, 7972 3. Xiangbing Zeng, Liliana Cseh, Georg H. Mehl and Goran Ungar, J. Mat. Chem., in press 4. B Glettner, F Liu, XB Zeng, M Prehm, U Baumeister, G Ungar, C Tschierske, Angew. Chem. Int. Ed., in press

Mesophase semiconductors: design for 3D-mesophases with effective paths for electronic charge hopping