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Simply grinding together metal salts and organic bridging ligands, in the absence of solvent in a shaker mill can provide crystalline, microporous metal-organic frameworks in only a few minutes and in quantitative yield[1]. Systematic studies of this unusual type of synthesis will be presented, including microscopy, structural templation by guests and by-products, the formation of interpenetrated structures, structures based on mixed-ligands, and the sorption characteristics of the resulting products. [1] Solvent-free synthesis of a microporous metal-organic framework, A. Pichon, A. Lazuen-Garay and S.L. James CrystEngComm 2006, 8, 211.

Application of the pair-distribution function method toin situstudies in catalysis