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In the field of polymer processing like injection moulding, film inflation and foaming, etc., the understanding of polymer deformation under shear and elongation is very important for the design of polymer with higher functionality. Especially in the film processing, deformation of polymer spherulite by drawing is the most interesting phenomenon and clarifying the deformation mechanism of spherulite will give a direction for better design of polymer film. Until now, to obtain the essential information about deformation behaviour of crystalline structure, many SAXS/WAXS researches about film deformation by drawing were reported by using synchrotron radiation X-rays. However, there is no report which focuses on the inhomogeneous deformation behaviour in one spherulite with a method of X-ray scattering. In this study, we try to obtain the information about local structure of one spherulite by using microbeam SAXS/WAXS technique.

Deformation process of polymer spherulite observed with microbeam-SAXS and -WAXS