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Ion irradiation experiments and quantitative x-ray diffraction analysis were used to demonstrate that the lattice and structure behave very differently in a complex oxide, $\ensuremath{\delta}\text{\ensuremath{-}}{\mathrm{Sc}}_{4}{\mathrm{Hf}}_{3}{\mathrm{O}}_{12}$, under irradiation. Analysis of the structure reveals that with increasing fluence, the characteristic $c/a$ ratio for the $\ensuremath{\delta}$ phase converges to that of an ideal fluorite phase, whereas locally it produces a metaphase consisting of frozen nanoscale structures having bixbyite-like flavor that increase the overall stability and radiation response of the apparent long-range oxygen-deficient average fluorite structure.

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Divergent short- and long-range behavior in ion-irradiated<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"><mml:mi>δ</mml:mi><mml:mo>−</mml:mo><mml:msub><mml:mi mathvariant="normal">Sc</mml:mi><mml:mn>4</mml:mn></mml:msub><mml:msub><mml:mi mathvariant="normal">Hf</mml:mi><mml:mn>3</mml:mn></mml:msub><mml:msub><mml:mi mathvariant="normal">O</mml:mi><mml:mn>12</mml:mn></mml:msub></mml:math>

Divergent short- and long-range behavior in ion-irradiatedδ−Sc4Hf3O12