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We present results of a coherent x-ray diffractive imaging experimentperformed on a single colloidal crystal grain. The full three-dimensional (3D)reciprocal space map measured by an azimuthal rotational scan contained severalorders of Bragg reflections together with the coherent interference signalbetween them. Applying the iterative phase retrieval approach, the 3D structureof the crystal grain was reconstructed and positions of individual colloidalparticles were resolved. As a result, an exact stacking sequence of hexagonalclose-packed layers including planar and linear defects were identified.

Revealing three-dimensional structure of individual colloidal crystal grain by coherent x-ray diffractive imaging