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Polar magnets are promising materials for new applications as multiferroics or in spintronics. In double corundum-related oxides, the cation ordering imposes a polar structure and the use of high pressure facilitates the insertion of magnetic cations into the compounds. Here we present the high-pressure synthesis of a new polar and ferrimagnetic corundum derivative Mn 2 InSbO 6 , which adopts the ordered-ilmenite-type structure. Neutron powder diffraction reveals that the high-temperature nearly collinear ferrimagnetic phase evolves to an incommensurate helical structure with k δ = [0 0 k z ] propagation vector, which then locks to the commensurate value of k z = 1/8. This complex magnetic behavior is likely to be related to magnetic frustration and the polar nature of the ordered double corundum structure.

physical review. b./physical review. b

Evolving spin periodicity and lock-in transition in the frustrated ordered ilmenite-type <mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML"><mml:mrow><mml:mi>β</mml:mi><mml:mtext>−</mml:mtext><mml:msub><mml:mi>Mn</mml:mi><mml:mn>2</mml:mn></mml:msub><mml:msub><mml:mi>InSbO</mml:mi><mml:mn>6</mml:mn></mml:msub></mml:mrow></mml:math>

Evolving spin periodicity and lock-in transition in the frustrated ordered ilmenite-type β−Mn2InSbO6