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Insulating 5d3 La3OsO7 and hole doped La2.8Ca0.2OsO7 materials featuring wellseparated pseudo-one-dimensional zig-zag chains of corner-sharing OsO6octahedra have been synthesized and their magnetic and electrical transportproperties characterized. Long range magnetic order between theantiferromagnetic chains is determined with a propagation vector k = 1/2, 1/2,0 and TN = 45 and 53 K for the parent and doped materials. An Os5+ moment of1.7(1) {\mu}B for La3OsO7 and 1.2(2) {\mu}B for La2.8Ca0.2OsO7 is refined. Thelong range magnetic structure is compared to the few currently known forisostructural Ln3MO7 compounds.

Magnetic Structure of the Quasi-One-Dimensional La3OsO7 as Determined by Neutron Powder Diffraction