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We studied the (001/2) diffraction peak in the low-temperature phase ofmagnetite (Fe3O4) using resonant soft x-ray diffraction (RSXD) at the Fe-L2,3and O-K resonance. We studied both molecular-beam-epitaxy (MBE) grown thinfilms and in-situ cleaved single crystals. From the comparison we have beenable to determine quantitatively the contribution of intrinsic absorptioneffects, thereby arriving at a consistent result for the (001/2) diffractionpeak spectrum. Our data also allow for the identification of extrinsic effects,e.g. for a detailed modeling of the spectra in case a "dead" surface layer ispresent that is only absorbing photons but does not contribute to thescattering signal.

Intrinsic and extrinsic x-ray absorption effects in soft x-ray diffraction from the superstructure in magnetite