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We report neutron diffraction experiments on the light-induced metastable state $S$I in single crystals of ${\mathrm{Na}}_{2}[\mathrm{Fe}{(\mathrm{CN})}_{5}\mathrm{NO}]∙2{\mathrm{D}}_{2}\mathrm{O}$. It is shown that the metastable state $S$I corresponds to a linkage isomer of the NO group, the so-called isonitrosyl configuration where the NO ligand is oxygen bound to the central iron atom.

physical review b

Neutron diffraction shows a photoinduced isonitrosyl linkage isomer in the metastable state<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:mi>S</mml:mi><mml:mi mathvariant="normal">I</mml:mi></mml:mrow></mml:math>of<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msub><mml:mi>Na</mml:mi><mml:mn>2</mml:mn></mml:msub><mml:mo>[</mml:mo><mml:mi>Fe</mml:mi><mml:msub><mml:mrow><mml:mo>(</mml:mo><mml:mi>CN</mml:mi><mml:mo…

Neutron diffraction shows a photoinduced isonitrosyl linkage isomer in the metastable stateSIofNa2[Fe(CN