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Mãssbauer isomer-shift measurements show that Yb is divalent in YbMo6S8• The asymmetry of the Yb thermal vibration at 4.2 K obtained from the Goldanskii-Karyagin effect is much smaller than that obtained from a Rietveld refinement of neutron powder diffraction data at 16 K. This suggests that the displacement of Yb off the origin includes a significant, -0.1-Á., static component which persists at low temperature. Full structural refinements at 16, 77, and 295 K show several interesting structural changes versus temperature.

physical review. b, condensed matter

Valence and delocalization of Yb in the Chevrel-phase Yb<mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant="normal">Mo</mml:mi></mml:mrow><mml:mrow><mml:mn>6</mml:mn></mml:mrow></mml:msub></mml:mrow></mml:math><mml:math xmlns:mml="http://www.w3.org/1998/Math/MathML" display="inline"><mml:mrow><mml:msub><mml:mrow><mml:mi mathvariant="normal">S</mml:mi></mml:mrow><mml:mrow><mml:mn>8</mml:mn></mml:mrow></mml:msub></mml:mrow…

Valence and delocalization of Yb in the Chevrel-phase YbMo6S8