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A pH-metric method for determining the acid values (AVs) of oilseeds in the range 0.6–10 mg KOH/g oil or more has been developed. The method is based on rapid (1–2 min) and complete extraction of free fatty acids from an oilseed test portion into a special reagent A, transfer of an aliquot of the reagent into pH-metric cell with another reagent B, and then measurement of the conditional pH in the mixture of reagents by a glass electrode. Total time for the determination including calculation is 9–10 min. The method is rapid, cheap, simple for automation, and not labor intensive.

pH-Metric Determination of the Acid Value of Oilseeds without Titration