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In this work, a new method was developed for perfluorinated compounds (PFCs) analysis in water samples based on decyl-perfluorinated magnetic mesoporous nanocomposites microspheres-assisted extraction and microwave-assisted derivatization followed by gas chromatography–mass spectrometry analysis. The decyl-perfluorinated magnetic mesoporous nanocomposites have several advantages such as fast separation ability, good dispersibility in water sample and high selective preconcentration of PFCs. Various parameters, including eluting solvent and volume, the amounts of absorbents, extraction time and elution time, the microwave-assisted derivatization conditions were optimized. Validation studies showed that this method has good linearity ( r  2  &gt; 0.9970), satisfactory precision (RSD &lt; 7.8%) and high recovery (93–107%). The limits of detection were found to be 0.055–0.086 μg/L and the limits of quantification be 0.18–0.28 μg/L, respectively. The results indicated that the proposed method has advantages of convenience, good sensitivity and high efficiency. The method has been applied successfully to analyze perfluorinated organic acids in real water samples.

journal of chromatographic science

Analysis of Perfluorinated Compounds in Environmental Water Using Decyl-perfluorinated Magnetic Mesoporous Microspheres as Magnetic Solid-Phase Extraction Materials and Microwave-Assisted Derivatization Followed by Gas Chromatography–mass Spectrometry