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Employing automated solid-phase microextraction—gas chromatography—selected ion monitoring-mass selective detection, mechanistic information on the formation of volatile components associated with carbonyl—amine chemistries in microwave heat-treated natural products is gathered. Employing  13 C uniformly labeled amino acids and sugars, pathways for the formation of Strecker aldehydes, pyrazines, and furan derivatives are delineated in a heat treated licorice suspension. The results are among the first pieces of information providing unambiguous reaction pathways for the production of these compounds in heated natural products.

Automated Solid-Phase Microextraction—Gas Chromatography—Mass Selective Detection Investigations of Carbonyl—Amine Reaction Pathways