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A method that uses solid-phase microextraction—gas chromatography—selected ion mode mass spectroscopy has been developed for the quantitative determination of phenolic compounds in cigarette smoke condensate. The concentrations of phenol,  o -,  m -, and  p -cresol, 2-methoxyphenol, 2,6-dimethylphenol, 2,4-dimethylphenol, 2,5-dimethylphenol, 4-ethylphenol, 3-ethylphenol, 2,4,6-trimethylphenol, 4-methoxyphenol, 3-methoxyphenol, vanillin, 1-napthol, and 2-napthol present in Kentucky Reference 2R1F and five commercial cigarette brands are determined. Minimal sample preparation is required, and no organic solvents or derivatization reagents are necessary.

journal of chromatographic science

Quantitative Determination of Phenols in Mainstream Smoke with Solid-Phase Microextraction-Gas Chromatography—Selected Ion Monitoring Mass Spectrometry