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The investigation was performed on pulse-electrodeposited Nickel with sub-microcrystalline microstructure containing slightly elongated grains having a fibre texture in growth direction. Structural units in form of groups of elongated grains possessing a common -zone axis in growth direction and CSL boundaries (in some cases twins) between them have been found in the microstructure by use of EBSD. Grain growth sets in above 325°C but the texture is conserved up to at least 600°C. This means that the arrangement of twins and other CSL boundaries stabilized the structural units; there is no orientation change (by further twinning) when grain growth occurs as seen in previous studies on Ni and Ni-Fe of different initial texture. The observed structural units were characterized in detail and the occurring grains and grain boundaries are described.

Characterization of multiple twinned structural units in pulse-electrodeposited nickel