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Perovskite lithium lanthanum titanate (LLTO) was prepared as an inorganic solid electrolyte material for lithium ion batteries applications using sol-gel method. Three different compositions of : (a) 3x=0.3 (Li  0.3 La  0.57 TiO 3 ), (b) 3x=0.5 (Li  0.5 La  0.5 TiO 3 ) were prepared and calcined at 1000°C for 6h, and (c) 3x=0.1 (Li  0.1 La  0.63 TiO 3 ) prepared and calcined at 1100°C for 6h. The effects of lithium content and calcination temperature on the structure of the perovskite powders were studied. The synthesized powders were characterized by X-ray diffraction analysis. Results indicate that the Li  0.3 La  0.57 TiO 3  was crystallized in tetragonal structure of space group P4/mmm. On the other hand, Rietveld refinement analysis for the LLTO samples confirmed the formation of the Li  0.3 La  0.57 TiO 3  crystalline phase in the tetragonal P4/mmm space group, the Li  0.5 La  0.5 TiO 3  phase in the tetragonal P4/mmm space group, and Li  0.1 La  0.63 TiO 3  phase in orthorhombic Pmmm space group.

iop conference series. materials science and engineering

Sol-gel synthesis and structural study of a lithium titanate phase Li 3xLa 2/3.x □1/3-2x TiO3 as solid electrolyte