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Recently developed instrumentation at the University of Washington hasallowed for nonresonant x-ray emission spectra (XES) to be measured in alaboratory-setting with an inexpensive, easily operated system. We present acritical evaluation of this equipment by means of K\b{eta} and valence-levelXES measurements for several Co compounds. We find peak count rates of ~5000/sfor concentrated samples and a robust relative energy scale withreproducibility of 25 meV or better. We furthermore find excellent agreementwith synchrotron measurements with only modest loss in energy resolution.Instruments such as ours, based on only conventional sources that are widelysold for elemental analysis by x-ray fluorescence, can fill an important roleto diversify the research applications of XES both by their presence innon-synchrotron laboratories and by their use in conjunction with XAFSbeamlines where the complementarity of XAFS and XES holds high scientificpotential.

Benchtop Nonresonant X-ray Emission Spectroscopy: Coming Soon to Laboratories and XAS Beamlines Near You?