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The design and construction of a sample holder for in operando X-ray absorption spectroscopy on solid oxide electrodes, like for instance the lanthanum strontium manganite electrodes, is explained. The sample holder is mounted in a test-cell, which is also described together with some preliminary test-results from temperature measurements and electrochemical characterisation performed on a "dummy" sample in the test cell. The test-cell is a modified version of a test-cell previously designed in our laboratory, and will in the future be used for X-ray absorption experiments on solid oxide electrodes.

Design of sample holder forin operandoXAS of oxidation state changes in La1−xSrxMnO3±δelectrodes

Design of sample holder forin operandoXAS of oxidation state changes in La_1−xSr_xMnO_3±δelectrodes