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HAADF-STEM tomography has been used to analyse the size and distribution of encapsulated gold nanoparticles (NPs) in hollow graphitised carbon nanofibres HAADF combined with a rolling-ball filter allows few-nm sized metallic NPs to be imaged with sufficient contrast against the higher volume carbon support structures to enable tomographic reconstruction

Analysis of few-nm sized metal nanoparticles on carbon nanostructures