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Nuclear inelastic scattering (NIS) spectra were recorded for thespin-crossover complexes STP and ETP (STP =[Fe(1,1,1-trisf[N-(2-pyridylmethyl)-N-methylamino]methylg- ethane)](ClO4)2 andETP =[Fe(1,1,1-trisf[N-(2-pyridylmethyl)-N-methylamino]methylg-butane)](ClO4)2) at30 K and at room temperature and also at ambient pressure and applied pressure(up to 2.6 GPa). Spin transition from the high-spin (HS) to the low-spin (LS)state was observed by lowering temperature and also by applying pressure atroom temperature and has been assigned to the hardening of iron-bond stretchingmodes due to the smaller volume in the LS isomer.

Pressure-induced changes of the vibrational modes of spin-crossover complexes studied by nuclear resonance scattering of synchrotron radiation