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We report the possibility to simultaneously perform wide-fieldnitrogen-vacancy (NV) diamond magnetic microscopy and synchrotron X-raydiffraction (XRD) measurements at high pressure. NV color centers are createdon the culet of a diamond anvil which is integrated in a diamond anvil cell forstatic compression of the sample. The optically detected spin resonance of theNV centers is used to map the stray magnetic field produced by the samplemagnetization. Using this combined scheme, the magnetic and structuralbehaviors can be simultaneously measured. As a proof-of-principle, we recordthe correlated {\alpha}-Fe to {\epsilon}-Fe structural and magnetic transitionsof iron that occur here between 15 and 20 GPa at 300 K.

Combined synchrotron X-ray diffraction and NV diamond magnetic microscopy measurements at high pressure