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We developed a new class of mono- or few-layered two-dimensional polymersbased on dinuclear (arene)ruthenium nodes, obtained by combining the iminecondensation with an interfacial chemistry process, and use a modifiedLangmuir-Schaefer method to transfer them onto solid surfaces. Robustnano-sheets of 2D polymers including dinuclear complexes of heavy rutheniumatoms as nodes were synthesised. These nano-sheets, whose thickness is of a fewtens of nanometers, were suspended onto solid porous membranes. Then, they werethoroughly characterised with a combination of local probes, including Ramanscattering, Fourier transform infrared spectroscopy and transmission electronmicroscopy in imaging and diffraction mode.

Nano-sheets of two-dimensional polymers with dinuclear (arene)ruthenium nodes, synthesised at a liquid/liquid interface