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The work represents a study of structure formation during thermally induced phase separation in low concentrated blends of semicrystalline polymers with thermodynamically poor solvents. According to the phase diagram, cooling of homogeneous blends located to the left of the upper critical solution temperature can cause two phase separation scenarios. The fact that both scenarios are possible is experimentally confirmed by investigating blends of polypropylene with a cosolvent and polyamide-12 with a cosolvent, using polarized light optical microscopy and scanning electron microscopy. The study proves the possibility to develop facile approaches to the formation of porous microspheres from semicrystalline polymers.

Formation of porous microspheres from semicrystalline polymer solutions: diffusion-controlled and local phase separation