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Rod-shaped and hexagon-like nanostructures of a phosphoric triamide 4-NO 2 C 6 H 4 C(O)NHP(O)(NHC(CH 3 ) 3 ) 2  have been prepared by a sonochemical method and a microwave process, respectively. The new nano-structures were characterized by SEM, XRD, UV–vis, infrared spectroscopy, and elemental analyses. The crystal structure of compound showed a distorted tetrahedral geometry for phosphorus with anti-configuration for the P(O) and C(O) groups respect to each other. Non-covalent interactions, that is, hydrogen bonding,stacking, and CH…HC contacts connected the chains into a 3D framework. Thermal stability in single crystalline and nano-scale was carried out by TGA and DSC. Further, P 2 O 5  nanosphericals have been prepared from a precursor nano-rod phosphoric triamide at 750 °C with a diameter of 30–40 nm. P 2 O 5  nanoparticles have been decorated from a single source precursor phosphoramide, 4-NO 2 C 6 H 4 C(O)NHP(O)(NHC(CH 3 ) 3 ) 2 , onto reduced graphen oxide surfaces by a solvothermal approach. Decorated nanoparticles have an orthorhombic phase with a sphere-like morphology and average size of 10–20 nm.

inorganic and nano-metal chemistry

Synthesis of phosphoric triamide nanostructures, characterization, X-ray crystallography, and preparation of P 2 O 5 -RGO nanocomposites by solvothermal method