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In this paper, sublimated AlCl 3  has been embedded on nanosilica-Fe 3 O 4  core via a simple method to obtain novel AlCl 3 @nano Fe 3 O 4 -SiO 2  nanostructure for the first time. The newly synthesized solid has been characterized by Fourier transformed infrared spectroscopy (FT-IR), field emission scanning electron microscopy (FESEM), energy dispersive X-ray spectroscopy (EDAX), vibrating sample magnetometer (VSM), transmission electron microscopy (TEM), X-ray diffraction analysis (XRD), Brunauer-Emmett-Teller (BET) measurements, and potentiometric titration techniques. The reactivity of the prepared nanoparticles was investigated in the synthesis of spiro[benzochromeno[2,3- d ]pyrimidin-indolines] through the one-pot three-component condensation of different naphthols, isatin derivatives, and barbituric acids in the in refluxing ethanol successfully. The recovery and reusability of the nanostructure has also been examined within 4 runs without activity loss.

inorganic and nano-metal chemistry

Novel AlCl 3 @nano Fe 3 O 4 -SiO 2 : a benign multi-layer magnetite nanocatalyst for the three-component one-pot synthesis of spiro[benzochromeno [2,3- d ]pyrimidin-indolines]