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A new Ni(II) and Pb(II) polymer [NiPb(dpdc)] n1  (H 2 dpdc = 2,6-dimethyl-pyridine-3,5-dicarboxylic acid) was synthesized under hydrothermal conditions. The compound crystallizes in the triclinic system, space group  P-1  with the final  R  = 0.0243 and  wR  = 0.0579 for 3590 observed reflections with  I  &gt; 2 σ ( I ). The compound presents a three-dimensional (3 D) network extended by dpdc 2-  anions employing a chelating coordination mode. From the topology point of view, the structure could be described as a (3,4)-connected 3 D network with (4.8.10)(8 2 .10) 2 (4.8.10 3 .12) topology net. Infrared spectroscopy, elemental analyses, thermogravimetric analysis and the single-crystal X-ray diffraction properties of  1  are also investigated.

Synthesis and crystal structure of a new three-dimensional Pb(II)/Ni(II) coordination polymer based on 2,6-dimethyl-pyridine-3,5-dicarboxylic acid