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A new compound, {[Co(TPA)(PYIM) 2 (H 2 O) 2 ](MI) 4 } n (1)(H 2 TPA = terephthalic acid, PYIM = 2-(3-pyridine) benzimidazole, MI = 2-lmidazolidone) has been urothermal synthesized and structurally characterized by elemental analysis, IR Spectra, the Powder Diffraction and single-crystal X-ray diffraction. Single-crystal X-ray diffraction analysis reveals that the (1 D)+(2D hydrogen bonds) pillar the compound 1 into an open 3 D supramolecular framework with a pore along the b axis (approximate dimensions 4.5 × 15 Å 2 ), which is occupied by free MI molecules. In addition, the catalytic-degradation capacity of compound 1 for methylene blue (MB) was investigated. Supplemental data for this article can be accessed online at 10.1080/24701556.2021.1916760

Synthesis, characterization, and degradation investigation of a novel (1D + 2D) coordination polymer