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Ag 3 PO 4 /BiPO 4  composite photocatalysts were constructed by a precipitation method. The composites were studied by Brunauer -Emmett-Teller (BET), X-ray diffraction patterns (XRD), UV-Vis diffuse reflectance spectra (DRS), scanning electron microscopy (SEM), high-resolution transmission electron microscopy (HRTEM), surface photovoltage spectroscopy (SPS), electron spin-resonance (ESR) spectroscopy and X-ray photoelectron spectroscopy (XPS). Ag 0  plays an important role in forming •O 2−  and accelerating the separation of the photo-induced charge pairs, consequently the Ag 3 PO 4 /BiPO 4  composites display high photocatalytic activity than the pure BiPO 4  under simulated sunlight irradiation. The separation and transfer of the photo-induced charge pairs abide by a Z-scheme mechanism.

Bridging role of Ag 0 particles formed in-situ on Ag 3 PO 4 /BiPO 4 composites for enhanced solar-driven photocatalytic performance