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The thermal analysis of the vertical Bridgman-grown In 2 Se 2.7 Sb 0.3  single crystals was carried out by recording the Thermogravimetric (TG), Differential Thermogravimetric (DTG), and Differential Thermal Analysis (DTA) curves. All three thermo-curves were recorded simultaneously by a thermal analyzer in the temperature range of ambient (300 K) to 923 K in the air atmosphere. The thermo-curves were recorded for single heating rates of 10 K/min. The thermal kinetic parameters of the vertical Bridgman-grown In 2 Se 2.7 Sb 0.3  single crystals were determined employing the non-mechanistic H-M (Horowitz and Metzger), P-N (Piloyan-Novikova), C-R (Coats-Redfem), and Broido relation from TGA and PRN (Piloyan, Ryabchikov, and Novikova) and BD (Borchardt and Daniels) relation from DTA curves. The determined kinetic parameters support the observations of the thermo-curves.

molecular crystals and liquid crystals

Thermal decomposition and kinetic parameter of Bridgman-grown In 2 Se 3−                                      x                  Sb                     x                   ( x  = 0.3) single crystal