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Two diiron toluene-3,4-dithiolate complexes with a phosphine ligand or a phosphite ligand were prepared and characterized. Treatment of complex [Fe 2 (CO) 6 { µ -SC 6 H 3 (CH 3 )S}] ( 1 ) with one equivalent of ethyldiphenylphosphine or methyldiphenylphosphinite and the decarbonylation agent Me 3 NO·2H 2 O gave analogues [Fe 2 (CO) 5 (Ph 2 PCH 2 CH 3 ){ µ -SC 6 H 3 (CH 3 )S}] ( 2 ) [Fe 2 (CO) 5 (Ph 2 POCH 3 ){ µ -SC 6 H 3 (CH 3 )S}] ( 3 ) and in 84% and 61% yields, respectively. Both analogues have been characterized by spectroscopy, elemental analysis, and X-ray crystallography. The electrochemical properties were probed by cyclic voltammetry.

molecular crystals and liquid crystals

Diiron toluene-3,4-dithiolate complexes with a phosphine ligand ethyldiphenylphosphine or a phosphite ligand methyldiphenylphosphinite: synthesis, characterization, X-ray crystal structures, and electrochemistry