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Six novel mixed-ligand complexes, [Cd(MCPA) 2 (bbhb)]n( 1 ), [Cd(MCPA) 2 (bib) 2 ]n( 2 ), [Co 2 (MCPA) 4 (pbix) 2 ] ( 3 ), [Zn(MCPA) 2 (pbix) 2 ]n( 4 ), [Cd(MCPA) 2 (obix) 2 ]n( 5 ), and [Co(MCPA) 2 (obix) 2 ]n( 6 ), have been synthesized under hydrothermal conditions and structurally characterized, where  MCPAH  = 2-methyl-4-chlorophenoxyacetic acid,  bbhb  = 1,1′-(1,4-butanediyl)bis-1 H -benzimidazole,  bib  = 1,4-bis(imidazol-1-yl)-butane,  pbix  = 1,4-bis(imidazol-1-ylmethyl)benzene and  obix  = 1,2-bis(imidazol-1-ylmethyl)benzene. X-ray diffraction analyses reveal that the N-donor ligands bridge the metal centers into different 1 D chains in complexes  1 ,  2 ,  4 ,  5,  and  6 , while  three  is a dinuclear molecule containing 26-membered ring. Furthermore, the luminescent properties of  1 ,  2 ,  4 , and  5  are also presented.

molecular crystals and liquid crystals

Syntheses, crystal structures, and properties of Zn(II), Cd(II), and Co(II) complexes based on 2-methyl-4-chlorophenoxyacetic acid and various N-donor ligands