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A light hydrogenation process involving the dissolution of zinc dust in diluted formic acid was developed to study the early hydrogenation stages of [Li@C 60 ] + PF 6-  and C 60 . The hydrogenation of the two substrates was followed through the electronic absorption spectroscopy and it was found that the metallofullerene reacts with hydrogen at least 2.4 times faster than C 60 , in line with theoretical expectations which suggest that [Li@C 60 ] is a better free radical acceptor than C 60 . The key absorption bands of the resulting fulleranes at low degree of hydrogen content were determined and discussed in an astrochemical perspective.

Hydrogenation of [Li@C 60 ]PF 6 : A comparison with fulleranes derived from C 60