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Six new compounds, xylomexicanins K-N ( 1 – 4 ), granasteroid ( 5 ) and 5-methoxy-2-pentylbenzofuran-7-ol ( 6 ), along with nine known compounds were isolated from the leaves and twigs of  Xylocarpus granatum . Among them,  1  was a biogenetic precursor of 1,8,9-phragmalin limonoid, and  4  represent the first example of degraded A-ring limonoid. The structures of them were elucidated on the basis of one- and two-dimensional NMR spectroscopic data (including  1 H,  13 C-NMR, DEPT,  1 H- 1 H COSY, HSQC, HMBC, and NOESY) and confirmed by high-resolution mass spectrometry.

Xylomexicanins K-N: limonoids from the leaves and twigs of Xylocarpus granatum