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In this study the porous composites, in-situ TiO 2 -g-C 3 N 4  (in-situ TiO 2 -g-CN), was fabricated by in-situ generation of TiO 2  from titanium tetra-oximate during thermal polymerisation of urea into gC 3 N 4 . For comparison, TiO 2 -g-C 3 N 4  composite (TiO 2 -g-CN) and g-C 3 N 4  (gCN) were also prepared by decomposition of urea in the presence and absence of TiO 2  nanoparticles (NPs), respectively. The synthesised composites were characterised by FT-IR, SEM-EDX, TGA, and XRD analyses. The analyses of the samples revealed that the particle size of the composites decreases with the addition of TiO 2  precursor, titanium tetra-oximate, during g-C 3 N 4  Synthesis. A comparative study has been conducted on the photocatalytic degradation of methylene blue (MB) and methyl orange (MO) dyes in the presence of in-situ TiO 2 -g-CN, TiO 2 -g-CN, and gCN under the solar spectrum. In the presence of in-situ TiO 2 -g-CN, 99.7% degradation of MB and 68.4% degradation of MO was observed within 100 min, and it is superior as compared to TiO 2 -g-CN and gCN.

Precursor-directed approach to fabricate TiO 2 -gCN composite: An efficient photocatalyst to harness solar spectrum