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In the recent decade, magnetic compounds have attracted a great deal of interest due to their magnetic behaviour allowing them to be a good candidate for catalytic and biomedical applications. However, the problem of these materials is their aggregation during the synthesis process, and then problems related to particle size. To overcome these problems, an efficient assembly of magnetic nanoparticles with layered double hydroxides compound systems ( Fe-NPs @LDH and  M/Fe-NPs @LDH; M = Mn, Zn) were prepared by simple co-precipitation process. Analytical tools including TG-dTG, XRD, FTIR, SEM/EDX and BET were used to investigate the thermal, morphological, structural and textural properties of the studied materials. The magnetic properties of the composite were investigated by mean  57 Fe Mossbauer spectrometry.

Synthesis of iron-based nanoparticles assembled with layered double hydroxides: structural and magnetic properties study