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The aim of the present paper is to develop of a new sol–gel synthesis route for production of phosphate-based glasses in TiO 2 -NiO-P 2 O 5  systems. The structure of the prepared glasses was investigated by ICP-AES, density methods, FTIR and RAMAN spectroscopy, XRD,  31 P MAS-NMR and DSC, that confirmed successful synthesis and production of phosphate-based glasses. Glasses in the TiO 2 - NiO- P 2 O 5  system with a high TiO 2  and NiO content of up to 12.5 mol% were synthesized in this study. XRD analysis confirms that all glass specimens with nickel are amorphous. Investigation of ternary glasses with the general formula of (70-x)TiO 2 -xNiO-30P 2 O 5 , whit x = 0, 2.5, 5, 7.5, 10 or 12.5 where revealed, substituting Nickel in place of titanium significantly extend the stability and prolongs the lifetime of these glasses, which opens else numerous of potential applications.

Elaboration and characterization of new glasses with high chemical durability in the system (70-x)TiO 2 -xNiO-30P 2 O 5