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Wide-angle X-ray scattering (WAXS) based upon synchrotron radiation is ideal for the  in situ  study of crystal structural changes during heating at high temperatures. This contribution describes a small furnace for  in situ  WAXS. The furnace has a wide coverage of scattered/diffracted angle from 0 to 135°, heats samples from room temperature to 1000 °C at 20 °C/min, and is suitable for  in situ  WAXS and radial distribution function of materials. Temperature calibration and safety verification are provided. The use of the furnace is demonstrated by  in situ  WAXS for the carbonization of bituminous coal.

Small, high temperature, wide-angle furnace for wide-angle X-ray scattering